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PM tool steels: microstructure, defects and Very High Cycle Fatigue
Karlstads universitet, Fakulteten för hälsa, natur- och teknikvetenskap (from 2013), Institutionen för ingenjörsvetenskap och fysik (from 2013).ORCID-id: 0009-0001-6982-3625
2025 (Engelska)Doktorsavhandling, sammanläggning (Övrigt vetenskapligt)
Abstract [en]

The martensitic tool steel grades are designed for various working environments. Their microstructure is continuously upgraded through composition development or processing techniques. These advancements introduce new types of defects, making fatigue response investigations critically important for industry.The present study includes the investigation of six advanced high strength tool steels in terms of microstructure, common defects, and fatigue performance in high and very high cycle fatigue regimes. The materials include: i) cold work tool steels (high alloyed materials manufactured via powder metallurgy processed by hot isostatic pressing and forging) and ii) hot work tool steels (conventionally produced by ingot cast and forging or additive manufacturing). Steel grades are compared based on strengths, martensitic structures, defect distributions, and fatigue strength using experimental results and the Murakami model. Also, a deeper analysis of the fatigue phenomena and mechanisms occurring during fatigue is attempted; characterization of fatigue initiation defects, the FGA, the fish-eye, as well as the crack propagation for the different microstructures are the main discussed subjects. The goal of the present study is to provide valuable insights to optimize martensitic tool steels for high and very high cycle fatigue applications.

Abstract [sv]

De martensitiska verktygsstålen är utformade för olika arbetsmiljöer. Deras mikrostruktur förbättras kontinuerligt genom utveckling av sammansättning eller bearbetningstekniker. Dessa framsteg introducerar nya typer av defekter, vilket gör undersökningar av utmattningsbeteende mycket viktiga för industrin.Den aktuella studien omfattar undersökningen av sex avancerade högstyrka verktygsstål med avseende på mikrostruktur, vanliga defekter och utmattningsprestanda i hög- och mycket högcykliska utmattningsområden. Materialen inkluderar: i) kallarbetsverktygsstål (höglegerade material tillverkade via pulvermetallurgi, bearbetade genom varm-isostatisk pressning och smidning) och ii) varmarbetsverktygsstål (konventionellt producerade genom gjutning av göt och smidning eller additiv tillverkning). Stålgraderna jämförs baserat på hållfasthet, martensitiska strukturer, defektfördelningar och utmattningshållfasthet med hjälp av experimentella resultat och Murakami-modellen. Dessutom görs en djupare analys av de utmattningsfenomen och mekanismer som uppträder under utmattning; karakterisering av initieringsdefekter, FGA, fisköga samt spricktillväxt för de olika mikrostrukturerna är de huvudsakliga ämnen som diskuteras.Målet med den aktuella studien är att ge värdefulla insikter för att optimera martensitiska verktygsstål för tillämpningar inom hög- och mycket högcyklisk utmattning.

Abstract [el]

Οι μαρτενσιτικοί εργαλειοχάλυβες είναι σχεδιασμένοι για να ανταπεξέρχονται σε περιβάλλονταυψηλών απαιτήσεων. Η μικροδομή τους συνεχώς βελτιώνεται διαφοροποιώντας είτε τη χημικήσύσταση του εκάστοτε συστήματος, είτε τη μέθοδο παρασκευής τους, ή τα βήματα που ακολοθούνταικατά την κατεργασία τους. Οι βελτιώσεις αυτές οδηγούν μεν σε προηγμένες μικροδομές, εισάγουνωστόσο νέους τύπους ατελειών, οι οποίες επηρεάζουν σε μεγάλο βαθμό την απόκρισή τους σε κυκλικήφόρτιση. Για αυτό το λόγο, η μελέτη της συμπεριφοράς τους σε κόπωση κρίνεται αναγκαία υπό τοπρίσμα της συνεχούς αύξησης των απαιτήσεων από τη μεριά της βιομηχανίας για υλικά που θααντέχουν όχι μόνο υψηλότερα φορτία, αλλά και για περισσότερο χρόνο. Τα υλικά που μελετώνται στην παρούσα εργασία περιλαμβάνουν:  i) εργαλειοχάλυβες ψυχρής κατεργασίας (υψηλά κραματωμένα υλικά που παράγονται μέσω κονεομεταλλουργίας και επεξεργάζονται με θερμή ισοστατική πίεση και σφυρηλάτηση) και ii) εργαλειοχάλυβες θερμής κατεργασίας (παραδοσιακά παραγόμενοι μέσω χύτευσης και σφυρηλάτησης ή Additive Μanufacturing). Οι εξί μικροδομές συγκρίνονται με βάση τη μικροδομή, την αντοχή σε κόπωση πολύ υψηλού αριθμού κύκλων,  την κατανομή και τους τύπους των ατελειών, χρησιμοποιώντας πειραματικά αποτελέσματα και το μοντέλο Murakami.Επιπλέον, επιχειρείται βαθύτερη ανάλυση των φαινομένων και μηχανισμών κόπωσης που λαμβάνουν χώρα κατά τη διάρκεια της κυκλικής φόρτισης. Ο χαρακτηρισμός των ατελειών που οδηγούν στη δημιουργία ρωγμής λόγω κόπωσης, της περιοχής FGA, του fish-eye καθώς και τους μηχανισμούς διάδοσης ρωγμών για τις διαφορετικές μικροδομές αποτελούν τα κύρια θέματα συζήτησης.

Ort, förlag, år, upplaga, sidor
Karlstads universitet, 2025. , s. 67
Serie
Karlstad University Studies, ISSN 1403-8099 ; 2025:46
Nyckelord [en]
High-strength tool steels, defects, fatigue response, VHCF regime
Nationell ämneskategori
Materialteknik
Forskningsämne
Materialteknik
Identifikatorer
URN: urn:nbn:se:kau:diva-107401DOI: 10.59217/jmom2393ISBN: 978-91-7867-635-4 (tryckt)ISBN: 978-91-7867-636-1 (digital)OAI: oai:DiVA.org:kau-107401DiVA, id: diva2:2010418
Disputation
2025-12-19, 21A342 (Eva Eriksson-salen), Karlstad University, Karlstad, 09:15 (Engelska)
Opponent
Handledare
Forskningsfinansiär
KK-stiftelsen, 20190033Tillgänglig från: 2025-11-28 Skapad: 2025-10-30 Senast uppdaterad: 2025-12-04Bibliografiskt granskad
Delarbeten
1. High and very high cycle fatigue behavior of an additive manufactured hot-work tool steel
Öppna denna publikation i ny flik eller fönster >>High and very high cycle fatigue behavior of an additive manufactured hot-work tool steel
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2024 (Engelska)Ingår i: Materials Science & Engineering: A, ISSN 0921-5093, E-ISSN 1873-4936, Vol. 917, artikel-id 147401Artikel i tidskrift (Refereegranskat) Published
Abstract [en]

In the present study, the fatigue response of an additive manufactured H13 type hot-work tool steel is investigated across the High Cycle Fatigue (HCF) and Very High Cycle (VHCF) regimes. The primary focus encompasses the interpretation of fatigue strength models, the defect type analysis along with a detailed examination of crack initiation and growth mechanisms. Despite the tremendous development in AM technology, experimental data regarding advanced mechanical properties, and particularly fatigue behavior, are still limited. Here, microstructural analysis of a modified AMed H13 hot-work tool steel, a combination of HCF and VHCF testing methodologies implemented for the characterization of the fatigue behavior, as well as a thorough fractographic analysis of the fractured surfaces were performed. Results are compared with historical data of a conventionally ingot cast and forged grade to assess the influence of the AM process on the fatigue response of H13 hot-work tool steels. It proves to be comparable to the conventionally manufactured grade, showcasing the potential utilization of AM in the production of components used in high-demanding applications, and in hot work tooling applications. However, the type of critical defects identified in the AM grade was found to be process-induced, emphasizing the need to optimize process parameters to reduce both the number and size of defects and also to ensure component reliability and high performance in various industrial applications. 

Ort, förlag, år, upplaga, sidor
Elsevier, 2024
Nyckelord
Fatigue crack, Fatigue testing, Fracture testing, High-cycle fatigue, Low-cycle fatigue, Metal working tools, Steel ingots, Steel testing, Thermal fatigue, AM h13 hot-work tool steel, Cycle fatigue behaviors, Fatigue behaviour, Fatigue response, Fatigue strength, High cycle, High cycle fatigue, Hot-work tool steel, Strength models, Very-High-Cycle Fatigue, Bessemer process
Nationell ämneskategori
Materialteknik
Forskningsämne
Materialteknik; Maskinteknik; Maskinteknik
Identifikatorer
urn:nbn:se:kau:diva-102151 (URN)10.1016/j.msea.2024.147401 (DOI)001339964900001 ()2-s2.0-85206614024 (Scopus ID)
Forskningsfinansiär
KK-stiftelsen, 20190033
Tillgänglig från: 2024-11-05 Skapad: 2024-11-05 Senast uppdaterad: 2025-10-30Bibliografiskt granskad
2. High-Nitrogen PM Tool Steel: A Comparison Of Microstructure And Mechanical Properties Of As-HIPed And HIPed Followed By Hot Working
Öppna denna publikation i ny flik eller fönster >>High-Nitrogen PM Tool Steel: A Comparison Of Microstructure And Mechanical Properties Of As-HIPed And HIPed Followed By Hot Working
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2022 (Engelska)Ingår i: World PM 2022 Congress Proceedings, European Powder Metallurgy Association (EPMA) , 2022Konferensbidrag, Publicerat paper (Övrigt vetenskapligt)
Abstract [en]

High-nitrogen-chromium alloyed powder metallurgy (PM) tool steels offer many attractive features including high strength and corrosion resistance. The PM route offers various advantages such as advanced alloy composition, high homogeneity, and well-defined size distribution of hard phase particles. This study presents microstructure and mechanical properties of a PM Cr-Mo-V-N alloy. The conventional manufacturing route for this alloy is hot isostatic pressing (HIP) followed by hot working. To investigate the possibility of near-net-shape manufacturing, a comprehensive comparison of the performance was made between steels produced by as-HIPed and HIPed followed by hot working. Both steel types were heat treated in the same way to obtain martensitic matrix with limited retained austenite. In the present investigation, microstructure and phase analyses were performed by X-ray diffraction and scanning electron microscopy. Mechanical tests were carried out by hardness measurements and tensile fatigue tests in the very high cycle fatigue regime using ultrasonic fatigue testing. 

Ort, förlag, år, upplaga, sidor
European Powder Metallurgy Association (EPMA), 2022
Nyckelord
Chromium alloys, Corrosion resistance, Corrosion resistant alloys, Fatigue testing, High strength alloys, High-cycle fatigue, Hot isostatic pressing, Microstructure, Molybdenum alloys, Molybdenum compounds, Scanning electron microscopy, Tensile testing, Tool steel, Ultrasonic testing, Advanced alloys, Alloy compositions, Alloyed powder, Hard phase, High homogeneity, High strength, Corrosion resistances, High-nitrogen, Microstructures, Mechanical properties, Phase particles; Size-distribution, Powder metallurgy
Nationell ämneskategori
Metallurgi och metalliska material Annan materialteknik
Forskningsämne
Materialteknik; Materialvetenskap
Identifikatorer
urn:nbn:se:kau:diva-95204 (URN)2-s2.0-85160795406 (Scopus ID)9781899072552 (ISBN)
Konferens
World PM 2022 Congress and Exhibition, Lyon, France, October 9-13, 2023.
Forskningsfinansiär
KK-stiftelsen, 20190033
Tillgänglig från: 2023-06-12 Skapad: 2023-06-12 Senast uppdaterad: 2025-11-17Bibliografiskt granskad
3. Very high cycle fatigue response and crack growth of a high-nitrogen-chromium powder metallurgy tool steel processed via hot isostatic pressing and hot working
Öppna denna publikation i ny flik eller fönster >>Very high cycle fatigue response and crack growth of a high-nitrogen-chromium powder metallurgy tool steel processed via hot isostatic pressing and hot working
(Engelska)Manuskript (preprint) (Övrigt vetenskapligt)
Abstract [en]

The present study aims to analyze the fatigue response and the crack growth rate of a high-nitrogen-chromium cold-work tool steel at the very high cycle fatigue regime. Detailed microstructural and fractographic analysis was conducted to examine the influence of the material´s highly alloyed martensitic microstructure on its fatigue response and crack growth damage at 20 kHz frequency. Fatigue testing was conducted under fully reversed cyclic loading (R= -1), while crack growth testing was performed in tensile-tensile cyclic loading (R= 0.1). The results revealed a fatigue strength of 691 MPa at 109 number of load cycles. Initiation points were of fish-eye type, i.e. inclusions of composition either directly connected to microstructure or pure oxides, and a fine granular area around the initiation defect. Regarding the crack growth behavior, the fractographic investigation revealed a strong influence of the stress intensity factor on the crack propagation microstructural features. A schematic interpretation of crack growth mechanisms as fine granular area formation, fish-eye crack growth, intra and trans martensite lath growth, and their relation to stress intensity levels were proposed.

Nyckelord
Very High Cycle Fatigue, Fatigue Crack Growth, High-nitrogen-chromium tool steel
Nationell ämneskategori
Annan materialteknik
Forskningsämne
Materialteknik
Identifikatorer
urn:nbn:se:kau:diva-107318 (URN)
Forskningsfinansiär
KK-stiftelsen, 20190033
Tillgänglig från: 2025-10-16 Skapad: 2025-10-16 Senast uppdaterad: 2025-10-30Bibliografiskt granskad
4. Microstructure, Defects and Fatigue Response of High Strength Tool Steels
Öppna denna publikation i ny flik eller fönster >>Microstructure, Defects and Fatigue Response of High Strength Tool Steels
(Engelska)Manuskript (preprint) (Övrigt vetenskapligt)
Abstract [en]

The martensitic tool steel family is designed for various working environments. Their microstructure is continuously upgraded through composition development or processing techniques. These advancements introduce new types of defects, making fatigue response investigations critically important for industry.

The present study includes the investigation of six advanced high strength tool steels in terms of microstructure, common defects, and fatigue performance in high and very high cycle fatigue regimes. The materials include: i) cold work tool steels (high alloyed materials manufactured via powder metallurgy processed by hot isostatic pressing and forging) and ii) hot work tool steels (conventionally produced by ingot cast and forging or additive manufacturing). Steel grades are compared based on strengths, martensitic structures, defect distributions, and fatigue strength using experimental results and the Murakami model. The goal of the present study is to provide valuable insights to optimize martensitic tool steels for high and very high cycle fatigue applications.

Nyckelord
High-strength tool steels, fatigue response, defects
Nationell ämneskategori
Metallurgi och metalliska material
Forskningsämne
Materialteknik
Identifikatorer
urn:nbn:se:kau:diva-107319 (URN)
Forskningsfinansiär
KK-stiftelsen, 20190033
Tillgänglig från: 2025-10-16 Skapad: 2025-10-16 Senast uppdaterad: 2025-10-30Bibliografiskt granskad
5. A case study of mechanical and thermal fatigue of press hardening dies
Öppna denna publikation i ny flik eller fönster >>A case study of mechanical and thermal fatigue of press hardening dies
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2022 (Engelska)Ingår i: IOP Conference Series: Materials Science and Engineering, 2022, Vol. 1238, nr 1, s. 1-10, artikel-id 012025Konferensbidrag, Publicerat paper (Refereegranskat)
Abstract [en]

Press hardening provides ultra-high strength steel components, typically boron steels, of complex geometries. In the process, the steel sheet is heated in a furnace to the austenitization temperature, transferred to the press, then simultaneously formed at high temperature and cooled in the die. Life limiting factors for the press hardening dies are mechanical fatigue, thermal fatigue, and wear. In the present case study two die segments were selected where critical damages were mechanical and thermal fatigue, respectively. The dies were made of a H13 type premium hot-work tool steel with complex heated die technology, die design integrating an advanced cooling system, for pressing automotive frame parts.

The first die failed due to mechanical loading with a crack initiated from the ejector pin area. The die design, the mechanical loads, the elevated temperature, and the tool steel crack resistance are main factors to consider. In the second die cracks initiated from an ejector pin hole, as well, due to thermal cycles causing alternating compressive and tensile stresses at the surface, which led to crack nucleation because of the accumulation of local plastic strain in the surface.

Nationell ämneskategori
Materialteknik
Forskningsämne
Materialteknik
Identifikatorer
urn:nbn:se:kau:diva-99227 (URN)10.1088/1757-899x/1238/1/012025 (DOI)
Konferens
International Deep-Drawing Research Group Conference (IDDRG 2022) 06/06/2022 - 10/06/2022 Lorient, France
Tillgänglig från: 2024-04-07 Skapad: 2024-04-07 Senast uppdaterad: 2025-10-30Bibliografiskt granskad

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Chantziara, Katerina

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