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  • 1. Abdel-Rehim, M.
    et al.
    Altun, Zeki
    Blomberg, Lars G
    Karlstad University, Faculty of Technology and Science, Department of Chemistry and Biomedical Sciences.
    New trend in sample preparation: On-line microextraction in packed syringe (MEPS) for LC and GC applications, Part II, Determination of ropivacaine and its metabolites in human plasma samples using MEPS-LC-MS-MS2004In: J. Mass Spectr., 39 (2004) 1488-1493Article in journal (Refereed)
  • 2. Abdel-Rehim, M.
    et al.
    Carlsson, Gunilla
    Karlstad University, Faculty of Health, Science and Technology (starting 2013), Paper Surface Centre. Karlstad University, Faculty of Technology and Science, Department of Chemistry and Biomedical Sciences. Karlstad University, Faculty of Technology and Science, Materials Science.
    Bielenstein, M.
    Arvidsson, T.
    Blomberg, Lars G
    Karlstad University, Faculty of Technology and Science, Department of Chemistry and Biomedical Sciences.
    Evaluation of Solid-Phase microextraction (SPME) for Study of the protein Binding in Human Plasma Samples,2000In: J. Chromatogr. Sci., 38 (2000) 458-464Article in journal (Refereed)
  • 3. Abdel-Rehim, M.
    et al.
    Hassan, Z.
    Blomberg, Lars G
    Karlstad University, Faculty of Technology and Science, Department of Chemistry and Biomedical Sciences.
    Hassan, M.
    Determination of Busulphan in plasma samples by gas chromatography-mass spectrometry (GC-MS) using on-line derivatization utilizing solid-phase microextraction (SPME)2003In: J. Therapeutic Drug Monitoring, 25 (2003) 400-406Article in journal (Refereed)
  • 4. Abdel-Rehim, M.
    et al.
    Skansen, P.
    Vita, M.
    Hassan, Z.
    Blomberg, Lars G
    Karlstad University, Faculty of Technology and Science, Department of Chemistry and Biomedical Sciences.
    Hassan, M.
    Microextraction in packed syringe / liquid chromatography /electrospray tandem mass spectrometry (MEPS/LC/MS/MS) for quantification of olomoucine in human plasma samples2005In: Anal.Chim. Acta., 539 (2005) 35-39Article in journal (Refereed)
  • 5.
    Abdel-Rehim, Mohamed
    et al.
    AstraZeneca R&D Södertälje, Södertälje, Sweden.
    Andersson, L.I.
    AstraZeneca R&D Södertälje, Södertälje, Sweden.
    Altun, Zeki
    Karlstad University, Faculty of Technology and Science, Department of Chemistry and Biomedical Sciences.
    Blomberg, Lars G
    Karlstad University, Faculty of Technology and Science, Department of Chemistry and Biomedical Sciences.
    Microextraction in Packed Syringe Online with Liquid Chromatography-Tandem Mass Spectrometry: Molecularly imprinted polymer as packing material for MEPS in selective extraction of ropivacaine from plasma2006In: Journal of Liquid Chromatography & Related Technologies, ISSN 1082-6076, E-ISSN 1520-572X, Vol. 29, no 12, p. 1725-1736Article in journal (Refereed)
    Abstract [en]

    The excellent performance of a new sample preparation method, microextraction in packed syringe (MEPS), was recently illustrated by online LC‐MS and GS‐MS assays of local anaesthetics in plasma samples. In the method, approximately 1 mg of solid packing material was inserted into a syringe (100–250 µL) as a plug. Sample preparation took place on the packed bed. The new method was easy to use, fully automated, of low cost, and rapid in comparison with previously used methods. This paper presents the use of molecularly imprinted polymers (MIPs) as packing material for higher extraction selectivity. Development and validation of a method for MIP‐MEPS online with LC‐MS‐MS using ropivacaine in plasma as model compound were investigated. A bupivacaine imprinted polymer was used. The method was validated and the standard curves were evaluated by means of quadratic regression and weighted by inverse of the concentration: 1/x for the calibration range 2–2000 nM. The applied polymer could be used more than 100 times before the syringe was discarded. The extraction recovery was 60%. The results showed high correlation coefficients (R 2 >0.999) for all runs. The accuracy, given as a percentage deviation from the nominal concentration values, ranged from -6% to 3%. The precision, given as the relative standard deviation, at three different concentrations (QC samples) was consistently about 3% to 10%. The limit of quantification was 2 nM.

  • 6. Abdel-Rehim, Mohamed
    et al.
    Dahlgren, Marie
    Blomberg, Lars G
    Karlstad University, Faculty of Technology and Science, Department of Chemistry and Biomedical Sciences.
    Quantification of ropivacaine and its major metabolites in human urine samples utilizing microextraction in packed syringe automated with liquid chromatography-tandem mass spectrometry (MEPS-LC-MS-MS)2006In: J. Sep. Sci., 29 (2006) 1658-1661Article in journal (Refereed)
  • 7. Abdel-Rehim, Mohamed
    et al.
    Dahlgren, Marie
    Claude, Saturnin
    Tabacchi, Raphael
    Blomberg, Lars G
    Karlstad University, Faculty of Technology and Science, Department of Chemistry and Biomedical Sciences.
    Microextraction in packed syringe (MEPS) utilizing methylcyanopropyl silarylene as coating polymer for extraction of drugs in biological samples,2006In: J. Liq. Chromatogr. & Relat. Technol., 29 (2006) No. 17, 2537-2544Article in journal (Refereed)
  • 8. Altun, Z.
    et al.
    Andersson, L.I.
    Blomberg, Lars G
    Karlstad University, Faculty of Technology and Science, Department of Chemistry and Biomedical Sciences.
    Abdel-Rehim, M.
    Some factors affecting the performance of microextraction in packed syringe (MEPS)2008In: submitted to Analyt. Chim. ActaArticle in journal (Refereed)
  • 9. Altun, Zeki
    et al.
    Abdel-Rehim, M.
    Blomberg, Lars G
    Karlstad University, Faculty of Technology and Science, Department of Chemistry and Biomedical Sciences.
    New trends in sample preparation: On-line microextraction in packed syringe (MEPS) for LC and GC applications. Part III Determination and validation of local anaesthetics in human plasma samples using a cation-exchange sorbent and MEPS-LC-MS-MS2004In: J. Chromatogr. B, 813 (2004) 129-135Article in journal (Refereed)
  • 10.
    Altun, Zeki
    et al.
    Karlstad University, Faculty of Technology and Science, Department of Chemistry and Biomedical Sciences.
    Andersson, Lars I.
    AstraZeneca R&D Södertälje, DMPK & BAC, Södertälje, Sweden.
    Blomberg, Lars G.
    Karlstad University, Faculty of Technology and Science, Department of Chemistry and Biomedical Sciences.
    Abdel-Rehim, Mohamed
    Karlstad University, Division for Business and Economics.
    Some Factors Affecting the Performance of Microextraction in Packed Syringe (MEPS)Manuscript (Other academic)
  • 11. Altun, Zeki
    et al.
    Blomberg, Lars G
    Karlstad University, Faculty of Technology and Science, Department of Chemistry and Biomedical Sciences.
    Use of carbon dioxide and ammonia as nebulizer gases in mass spectrometry2002In: Rapid Comm. Mass Spectrometry, 16 (2002) 738-739Article in journal (Refereed)
  • 12.
    Altun, Zeki
    et al.
    Karlstad University, Division for Chemistry.
    Blomberg, Lars G.
    Karlstad University, Division for Chemistry.
    Abdel-Rehim, Mohamed
    Karlstad University, Division for Chemistry.
    Increasing Sample Preparation Throughput Using Monolithic Methacrylate Polymer as Packing Material for 96-Tips: 2 Minutes per 96-Well Plate2005Manuscript (preprint) (Other academic)
  • 13. Altun, Zeki
    et al.
    Hjelmström, Anette
    Abdel-Rehim, Mohamed
    Blomberg, Lars G
    Karlstad University, Faculty of Technology and Science, Department of Chemistry and Biomedical Sciences.
    Surface Modified Polypropylene Pipette Tips Packed with a Monolithic Plug of Adsorbent for High Throughput Sample Preparation2007In: J. Sep. Sci., 30 (2007) 1964-1972Article in journal (Refereed)
  • 14. Altun, Zeki
    et al.
    Hjelmström, Anette
    Blomberg, Lars G
    Karlstad University, Faculty of Technology and Science, Department of Chemistry and Biomedical Sciences.
    Abdel-Rehim, Mohamed
    Evaluation of monolithic packed 96-tips for solid-phase extraction of local anesthetics from human plasma for quantitation by liquid chromatography tandem mass spectrometry2008In: J. Liq. Chromatogr. & Relat. Technol , 31 (2008) 743-751Article in journal (Refereed)
  • 15. Altun, Zeki
    et al.
    Jagerdeo, E.
    Blomberg, Lars G
    Karlstad University, Faculty of Technology and Science, Department of Chemistry and Biomedical Sciences.
    Abdel-Rehim, M.
    Drug screening using microextraction in packed syringe (MEPS) / LC-MS utilizing monolithic-based sorbent material,2006In: Journal of Liquid Chromatography and Related Technologies, 29 (2006) 829-839Article in journal (Refereed)
  • 16. Andersson, Magnus
    et al.
    Lu, B.
    Abdel-Rehim, M.
    Blomberg, S.
    Blomberg, Lars G
    Karlstad University, Faculty of Technology and Science, Department of Chemistry and Biomedical Sciences.
    Capillary electrophoresis methods for the separation of the basic compound lidocaine and its metabolites2004In: Rapid Commun. Mass Spectr., 18 (2004) 2612-2618Article in journal (Refereed)
  • 17. Andersson, Magnus
    et al.
    Wan, H.
    Abdel-Rehim, M.
    Blomberg, Lars G
    Karlstad University, Faculty of Technology and Science, Department of Chemistry and Biomedical Sciences.
    Characterization of Lidocaine and its Metabolites in Human Plasma using Capillary Electrophoresis,1999In: J. Microcol. Sep., 11, (1999) 620-626Article in journal (Refereed)
  • 18. Andersson, M.B.O.
    et al.
    Blomberg, Lars G
    Karlstad University, Faculty of Technology and Science, Department of Chemistry and Biomedical Sciences.
    Electric field-assisted micro-packed HPLC,2001In: J. Sep. Sci. 24 (2001) 304-308Article in journal (Refereed)
  • 19. Andersson,, M.B.O.
    et al.
    King, J.W.
    Blomberg, Lars G
    Karlstad University, Faculty of Technology and Science, Department of Chemistry and Biomedical Sciences.
    Synthesis of fatty alcohol mixtures from oleochemicals in supercritical fluids,2000In: Green Chemistry, (2000) 230-234Article in journal (Refereed)
  • 20.
    Blomberg, Lars G
    Karlstad University, Faculty of Technology and Science, Department of Chemistry and Biomedical Sciences.
    Analysis of fatty acids by capillary electrophoresis,1999In: Lipid Technology, 11, (1999) 140-142Article in journal (Refereed)
  • 21.
    Blomberg, Lars G
    Karlstad University, Faculty of Technology and Science, Department of Chemistry and Biomedical Sciences.
    Current Aspects of Stationary Phases for Gas Chromatography, (Guest editorial)1998In: LC/GC Int., 11 (1998) 760-762Article in journal (Refereed)
  • 22.
    Blomberg, Lars G
    Karlstad University, Faculty of Technology and Science, Department of Chemistry and Biomedical Sciences.
    Effects and nature of buffer ion enrichment in electrical field assisted liquid chromatography2004Licentiate thesis, monograph (Other academic)
  • 23.
    Blomberg, Lars G
    Karlstad University, Faculty of Technology and Science, Department of Chemistry and Biomedical Sciences.
    In-line application of electric field in capillary separation systems2006Doctoral thesis, monograph (Other academic)
  • 24.
    Blomberg, Lars G
    Karlstad University, Faculty of Technology and Science, Department of Chemistry and Biomedical Sciences.
    Models in chemistry education - A study of teaching and learning acids and bases in Swedish upper secondary schools2007Doctoral thesis, monograph (Other academic)
  • 25.
    Blomberg, Lars G
    Karlstad University, Faculty of Technology and Science, Department of Chemistry and Biomedical Sciences.
    Professional supervision of doctoral education in science2010In: Strömstad akademi, Vision och verklighet / [ed] A. Ott och C.E. Olivestam, Strömstad: Strömstad akademi , 2010, p. 91-112Chapter in book (Other academic)
  • 26.
    Blomberg, Lars G
    Karlstad University, Faculty of Technology and Science, Department of Chemistry and Biomedical Sciences.
    Silicone stationary phases for gas chromatography,2001In: LC/GC Europe, 14 (2001) 106-112Article in journal (Refereed)
  • 27.
    Blomberg, Lars G
    Karlstad University, Faculty of Technology and Science, Department of Chemistry and Biomedical Sciences.
    Textbooks, teachers, and students understanding of models used to explain acid-base reactions2005Licentiate thesis, monograph (Other academic)
  • 28.
    Blomberg, Lars G
    Karlstad University, Faculty of Technology and Science, Department of Chemistry and Biomedical Sciences.
    Two new techniques for sample preparation in bioanalysis: Microextraction in packed sorbent (MEPS) and use of a bonded monolith as sorbent for sample preparation in polypropylene tips for 96-well plates2009In: Analytical and Bioanalytical Chemistry, ISSN 1618-2642, E-ISSN 1618-2650, Vol. 393, no 3, p. 797-807Article in journal (Refereed)
  • 29.
    Blomberg, Lars G
    et al.
    Karlstad University, Faculty of Technology and Science, Department of Chemistry and Biomedical Sciences.
    Abdel-rehim, M
    Current advances in microextraction by packed sorbent (MEPS) for bioanalysis applications2009In: LCGC Europé, ISSN 1471-6577, Vol. 22, no 1, p. 8-19Article in journal (Refereed)
  • 30.
    Blomberg, Lars G
    et al.
    Karlstad University, Faculty of Technology and Science, Department of Chemistry and Biomedical Sciences.
    Abdel-Rehim, M
    Recent advances in microextraction by packed sorbent for bioanalysis2010In: Journal of Chromatography A, ISSN 0021-9673, E-ISSN 1873-3778, Vol. 1217, no 16, p. 2569-2580Article in journal (Refereed)
  • 31.
    Blomberg, Lars G
    et al.
    Karlstad University, Faculty of Technology and Science, Department of Chemistry and Biomedical Sciences.
    Abdel-Rehim, M.
    Askemark, Y.
    Norsten-Höög, C.
    Pettersson, K-J.
    Halldin, M.
    Quantification of 4-OH-2,6-Xylidine and its Conjugates in Human Urine Samples Utilising Microextraction in Packed Syringe On-line with Liquid Chromatography and Electrospray Tandem Mass Spectrometry (MEPS-LC-MS/MS)2006In: J. Liq. Chromatogr. & Relat. Technol., 29 (2006) (16), 2413-2424Article in journal (Refereed)
  • 32.
    Blomberg, Lars G
    et al.
    Karlstad University, Faculty of Technology and Science, Department of Chemistry and Biomedical Sciences.
    Abdel-Rehim, M.
    Askemark, Y.
    Norsten-Höög, C.
    Pettersson, K-J.
    Halldin, M.
    Quantification of 4-OH-2,6-Xylidine and its Conjugates in Human Urine Samples Utilising Microextraction in Packed Syringe On-line with Liquid Chromatography and Electrospray Tandem Mass Spectrometry (MEPS-LC-MS/MS)2006In: J. Liq. Chromatogr. & Relat. Technol., 29 (2006) (16), 2413-2424Article in journal (Refereed)
  • 33.
    Blomberg, Lars G
    et al.
    Karlstad University, Faculty of Technology and Science, Department of Chemistry and Biomedical Sciences.
    Abdel-Rehim, M.
    Askemark, Y.
    Norsten-Höög, C.
    Pettersson, K-J.
    Halldin, M.
    Quantification of 4-OH-2,6-Xylidine and its Conjugates in Human Urine Samples Utilising Microextraction in Packed Syringe On-line with Liquid Chromatography and Electrospray Tandem Mass Spectrometry (MEPS-LC-MS/MS)2006In: J. Liq. Chromatogr. & Relat. Technol., 29 (2006) (16), 2413-2424Article in journal (Refereed)
  • 34.
    Blomberg, Lars G
    et al.
    Karlstad University, Faculty of Technology and Science, Department of Chemistry and Biomedical Sciences.
    Abdel-Rehim,, Mohamed
    Andersson,, Anita
    Breitholtz-Emanuelsson, Anna
    Sandberg-Ställ, Maria
    Brunfelter, Kristina
    Pettersson, Karl-Johan
    Norsten-Höög, Carina
    Microextraction in packed syringe (MEPS) as a rapid sample preparation method to handle unstable compounds in a complex matrix: Determination of AZD3409 in plasma samples utilizing microextraction in packed syringe and liquid chromatography-tandem mass sp2008In: J. Chromatog. Sci., acceptedArticle in journal (Refereed)
  • 35.
    Blomberg, Lars G
    et al.
    Karlstad University, Faculty of Technology and Science, Department of Chemistry and Biomedical Sciences.
    Abdel-Rehim, Mohamed
    Hassan, Zuzana
    Skansen, Patrik
    Hassan, Moustapha
    Microextraction in packed syringe / liquid chromatography /electrospray tandem mass spectrometry (MEPS/LC/MS/MS) for quantification of busulfan in human plasma samples2007In: J. Liq. Chromatogr. & Relat. Technol., 30 (2007) 3029-3041Article in journal (Refereed)
  • 36.
    Blomberg, Lars G
    et al.
    Karlstad University, Faculty of Technology and Science, Department of Chemistry and Biomedical Sciences.
    Altun, Z.
    Abdel-Rehim, M.
    Study of the factors affecting the performance of microextraction by packed sorbent (MEPS) using liquid scintillation counter and liquid chromatography-tandem mass spectrometry2008In: Analytica Chimica Acta, 630, 116-123Article in journal (Refereed)
  • 37.
    Blomberg, Lars G
    et al.
    Karlstad University, Faculty of Technology and Science, Department of Chemistry and Biomedical Sciences.
    Altun, Zeki
    New Techniques for Sample Preparation in Analytical Chemistry2005Licentiate thesis, monograph (Other academic)
  • 38.
    Blomberg, Lars G
    et al.
    Karlstad University, Faculty of Technology and Science, Department of Chemistry and Biomedical Sciences.
    Altun, Zeki
    New Techniques for Sample Preparation in Analytical Chemistry - Micro Extraction in Packed Syringe (MEPS) and Methacrylate Based Monolithic Pipette Tips2008Doctoral thesis, monograph (Other academic)
  • 39.
    Blomberg, Lars G
    et al.
    Karlstad University, Faculty of Technology and Science, Department of Chemistry and Biomedical Sciences.
    Altun, Zeki
    Altun, Z.
    Abdel-Rehim, M.
    Increasing Sample Preparation Throughput Using Monolithic Methacrylate Polymer as Packing Material for 96-Tips2006In: J. Chromatogr. B, J. Liq. Chromatogr. & Rel. Technol., 29 (2006) 1725-1736Article in journal (Refereed)
  • 40.
    Blomberg, Lars G
    et al.
    Karlstad University, Faculty of Technology and Science, Department of Chemistry and Biomedical Sciences.
    Altun, Zeki
    Karlstad University, Faculty of Technology and Science, Department of Chemistry and Biomedical Sciences.
    Skoglund, C
    Abdel-Rehim, M
    Monolithic methacrylate packed 96-tips for high throughput bioanalysis2010In: Journal of Chromatography A, ISSN 0021-9673, Vol. 1217, no 16, p. 2581-2588Article in journal (Refereed)
  • 41.
    Blomberg, Lars G
    et al.
    Karlstad University, Faculty of Technology and Science, Department of Chemistry and Biomedical Sciences.
    Andersson, Magnus
    Abdel-Rehim, M.
    Portelius, E.
    Norsten-Höög, C.
    Determination of Ropivacaine and its metabolites in Human Plasma Using Solid Phase Microextraction and GC-NPD / GC-MS2001In: J. Microcol. Sep. 13 (2001) 313-321Article in journal (Refereed)
  • 42.
    Blomberg, Lars G
    et al.
    Karlstad University, Faculty of Technology and Science, Department of Chemistry and Biomedical Sciences.
    Bohlin, Maria E.
    Capillary electrophoresis of 2-glycoprotein I: method development and binding studies2006Licentiate thesis, monograph (Other academic)
  • 43.
    Blomberg, Lars G
    et al.
    Karlstad University, Faculty of Technology and Science, Department of Chemistry and Biomedical Sciences.
    El-BeqqalI, Aziz
    Kussak, Anders
    Abdel-Rehim, Mohamed
    Fast and sensitive environmental analysis utilizing microextraction in packed syringe online with gas chromatography-mass spectrometry. Determination of polycyclic aromatic hydrocarbons in water2006In: J. Chromatogr. A, 1114 (2006) 234-238Article in journal (Refereed)
  • 44.
    Blomberg, Lars G
    et al.
    Karlstad University, Faculty of Technology and Science, Department of Chemistry and Biomedical Sciences.
    El-Beqqali, Aziza
    Abdel-Rehim, Mohamed
    Quantitative analysis of methadone in human urine samples by microextraction in packed syringe-gas chromatography-mass spectrometry (MEPS-GC-MS)2007In: J. Sep. Sci. 30 (2007) 2501-2505Article in journal (Refereed)
  • 45.
    Blomberg, Lars G
    et al.
    Karlstad University, Faculty of Technology and Science, Department of Chemistry and Biomedical Sciences.
    El-Beqqali, Aziza
    Abdel-Rehim, Mohamed
    Use of carbon dioxide as collision gas in tandem mass spectrometry2005In: Rapid Commun. Mass Spectr., 19 (2005) 2099-2102Article in journal (Refereed)
  • 46.
    Blomberg, Lars G
    et al.
    Karlstad University, Faculty of Technology and Science, Department of Chemistry and Biomedical Sciences.
    El-Beqqali, Aziza
    Kussak, Anders
    Abdel-Rehim, Mohamed
    Determination of dopamine and serotonine in human urine samples utilizing microextraction online with liquid chromatography /electrospray tandem mass spectrometry2007In: J. Sep. Sci. 30 (2007) 421-424Article in journal (Refereed)
  • 47.
    Blomberg, Lars G
    et al.
    Karlstad University, Faculty of Technology and Science, Department of Chemistry and Biomedical Sciences.
    Jagerdeo, E
    Abdel-Rehim, M
    Sreening of cocaine and its metabolites in human urine samples by direct analysis in real-time sourse coupled to time-of-flight mass spectrometry after online preconcentration utilizing microextraction by packed sorbent2009In: Journal of the American Society for Mass Spectrometry, ISSN 1044-0305, E-ISSN 1879-1123, Vol. 20, no 5, p. 891-899Article in journal (Refereed)
  • 48.
    Blomberg, Lars G
    et al.
    Karlstad University, Faculty of Technology and Science, Department of Chemistry and Biomedical Sciences.
    Magnusson, Jeanette
    Evaluation of modified cyclodextrins for chiral separations in gas chromatography and capillary electrophoresis2002Licentiate thesis, monograph (Other academic)
  • 49.
    Blomberg, Lars G
    et al.
    Karlstad University, Faculty of Technology and Science, Department of Chemistry and Biomedical Sciences.
    Onnerud, H
    Bassiouny, F
    Abdel-Rehim, M
    Chromatographic behaviour of bupivacaine and five of its major metabolites in human plasma, utilizing solid-phase extraction and capillary gas chromatography2010In: Journal of Chromatographic Science, ISSN 0021-9665, E-ISSN 1945-239X, Vol. 48, no 4, p. 294-298Article in journal (Refereed)
  • 50.
    Blomberg, Lars G
    et al.
    Karlstad University, Faculty of Technology and Science, Department of Chemistry and Biomedical Sciences.
    Said, Rana
    Abdel-Rehim, Mohamed
    Whole blood analysis utilizing microextraction by packed sorbent (MEPS) on-line with liquid chromatography-tandem mass spectrometry (LC-MS/MS)2008In: Submitted to J. Chromatogr. BArticle in journal (Refereed)
12 1 - 50 of 91
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